BP609PSemester 62 creditsPractical
Pharmaceutical Analysis (Practical)
Complete unit-wise syllabus for BP609P as per the PCI B.Pharm NEP 2020 curriculum (Semester 6 — AI in Pharma + Analysis + Internship II).
URL:
https://pharmacode.vercel.app/syllabus/semester-6/bp609p-pharmaceutical-analysis-practical/Course Objectives
- Understand the fundamental principles behind various analytical techniques including titrations, spectrophotometry, fluorimetry, flame photometry, and chromatography.
- Develop proficiency in performing quantitative and qualitative analyses of pharmaceutical compounds using classical and instrumental methods.
- Learn to operate and maintain laboratory instruments such as potentiometers, conductometers, spectrophotometers, fluorimeters, flame photometers, and chromatographic systems.
- Apply appropriate analytical techniques for specific analytical challenges and interpretation, including single and multi-component assays, identification of functional groups, and separation of mixtures.
- Learn good laboratory practices and safety protocols in handling chemicals and operating instruments.
Unit-wise Syllabus
1 Units1
Laboratory Practicals & Experiments (60 Hours)60 Hours- 1. Determination of the endpoint of a acid base titration by potentiometric method.
- 2. Determination of end point of acid base titrations by conductometry.
- 3. Determination of absorption maxima and effect of solvents on absorption maxima of organic compounds
- 4. Assay of APIs by colorimetry.
- 5. Assay of single component by UV- Spectrophotometer.
- 6. Simultaneous estimation of multicomponent formulations by UV spectrophotometer.
- 7. Identification of various functional groups in official compounds by FTIR as per IP.
- 8. Assay of quinine sulphate by fluorimetry
- 9. Determination of quenching effect by fluorimetry
- 10. Assay of sodium chloride by flame photometry
- 11. Assay of potassium chloride by flame photometry
- 12. Determination of chlorides and sulphates by nephelo turbidometry
- 13. Separation of amino acids by paper chromatography
- 14. Separation of mixture of components by thin layer chromatography
- 15. Demonstration experiment on GC
- 16. Determination of official compounds by HPLC (anyone)
- 17. Demonstration experiment on HPTLC.
Get complete notes for BP609P
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Recommended Textbooks & References
- Vogel, A.I., Textbook of Quantitative Chemical Analysis. Longman Scientific & Technical.
- Beckett, A.H., and Stenlake, J.B., Practical Pharmaceutical Chemistry: Part II. Athlone Press.
- Skoog, D.A., Holler, F.J., and Crouch, S.R., Principles of Instrumental Analysis. Cengage Learning.
What's coming next on this page
- Previous year question papers (PYQ)
- Topic-wise short notes and revision summaries
- MCQs and self-assessment quizzes
- Suggested external resources and video tutorials
Other subjects in Semester 6
BP601TAdvanced PharmacognosyBP602TBiopharmaceutics and PharmacokineticsBP603TIntellectual Property RightsBP604TAI Applications in Pharmaceutical SciencesBP605TPharmaceutical AnalysisBP606TPharmaceutical JurisprudenceBP607T AECAEC Elective — Green Chemistry / Materiovigilance / Scientific Writing / Drug Store Management / Medicinal Plant Cultivation / API SciencesBP608PBiopharmaceutics and Pharmacokinetics (Practical)BP610P SECSEC Elective — Computer-Aided Drug Design / Analytical Method Development / Principles of Preclinical Studies (Practical)BP611P VACVAC Elective — Professional Skills / Process Analytical Technology & Quality by Design (Practical)BP612IInternship II (Mandatory)