BP709PSemester 71 creditsPractical
Modern Analytical Techniques (Practical)
Complete unit-wise syllabus for BP709P as per the PCI B.Pharm NEP 2020 curriculum (Semester 7 — Pharmacovigilance + Regulatory + Research).
URL:
https://pharmacode.vercel.app/syllabus/semester-7/bp709p-modern-analytical-techniques-practical/Course Objectives
- Provide practical training in interpretation of advanced instrumental data used for structural and physicochemical characterization.
- Introduce quantitative analytical techniques using modern separation methods, such as UHPLC and HPLC, for the estimation of pharmaceutical substances.
- Familiarize students with the principles and practice of green analytical chemistry, including preparation of green solvents and development of environmentally sustainable analytical methods.
- Develop understanding of bioanalytical sample preparation techniques for pharmaceutical analysis in biological matrices, including solid phase extraction, liquid– liquid extraction, and protein precipitation.
- Learn applied pharmaceutical analysis and methods including cell viability assays, residual solvent analysis, and estimation of drugs from biological fluids.
Unit-wise Syllabus
1 Units1
Laboratory Practicals & Experiments (45 Hours)45 Hours- 1. Interpretation of Proton NMR spectra of known compound (any two)
- 2. Interpretation of Carbon NMR spectra of known compound (any two)
- 3. Interpretation of mass spectrum of known compound (any two)
- 4. Interpretation of X-Ray diffraction spectrum (any one)
- 5. Interpretation of DSC Thermogram (any one)
- 6. Preparation and Evaluation of Green Analytical Solvents
- 7. Analytical method development by using Green chemistry
- 8. Quantification of pharmaceuticals in biological fluids using Solid Phase Extraction (SPE)
- 9. Quantification of pharmaceuticals in biological matrix by PPE
- 10. Quantification of pharmaceuticals in biological matrix by LLE
- 11. Demonstration of Cell Viability evaluation using MTT Assay
- 12. Demonstration on residual solvent analysis using GC
- 13. Assay of drug using HPLC (any two)
- 14. Analysis of drug from biological fluid using HPLC/ UV spectroscopy.
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Recommended Textbooks & References
- 1. Beckett, A. H. and Stenlake, J. B. Practical Pharmaceutical Chemistry. CBS Publishers & Distributors.
- Brittain, H. G. Analytical Profiles of Drug Substances and Excipients. Elsevier.
- Kemp, W. Organic Spectroscopy. Palgrave Macmillan.
- Munson, J. W. Pharmaceutical Analysis: Modern Methods. Marcel Dekker.
- Sharma, Y. R. Organic Spectroscopy. S. Chand.
- Silverstein, R. M., Webster, F. X., Kiemle, D. J. and Bryce, D. L. Spectrometric Identification of Organic Compounds. Wiley.
- Willard, H. H., Merritt, L. L., Dean, J. A. and Settle, F. A. Instrumental Methods of Analysis. Brooks/Cole.
- Indian Pharmacopoeia. Indian Pharmacopoeia Commission.
What's coming next on this page
- Previous year question papers (PYQ)
- Topic-wise short notes and revision summaries
- MCQs and self-assessment quizzes
- Suggested external resources and video tutorials
Other subjects in Semester 7
BP701TBiostatistics Research MethodologyBP702TCosmetics and CosmeceuticalsBP703TAI in Clinical ApplicationsBP704TModern Analytical TechniquesBP705TPharmacovigilanceBP706TPharmacy PracticeBP707TRegulatory AffairsBP708T AECAEC Elective — Current Good Manufacturing Practices / Pharmaceutical Automation / Cellular Biology / Medical Devices / Food Waste Products / BiosimilarsBP710RPResearch Project (Major)